Quality Control

QCX/RoboLab

A typical QCX/RoboLab® configuration consists of a standard industrial robot placed in the centre of a circular arrangement of sample preparation and analytical equipment.

  • Concepts
  • Application
  • Functionality

Concepts

A typical QCX/RoboLab configuration consists of a standard industrial robot placed in the centre of a circular arrangement of sample preparation and analytical equipment. Samples normally arrive automatically from the connected automatic sample transport system, but may also be entered via operator sample conveyors or special input/output magazines.

QCX/RoboLab offers a very high flexibility in terms of the number and types of equipment handled by the robot. Supported, fully automated preparation & analysis disciplines relevant to the cement industry include powder or fused bead preparation for X-ray analysis, particle sizing by laser or by conventional sieving, colour analysis, Carbon/Sulphur/Moisture combustion analysis, physical testing and collection of shift/daily composites. For the typical cement lab project a throughput capacity of 10-20 samples will apply; but higher numbers in one robot cell are achievable.

QCX/RoboLab is one of two alternative laboratory automation concepts available from FLSmidth; the other is QCX/AutoPrep. These two automation solutions are exponents from each of the following two main categories of automation concepts for sample preparation and analysis :  

  • Automated equipment systems: Laboratories in which the sample preparation units and the analysis equipment are automated and then linked together by conventional transport belts or the alike. The automation is provided by dedicated highly specialised equipment units. 
  • Robotics systems: Laboratories in which automation is achieved by robotics. The equipment units serviced by the robot(s) may be fully automated, semi-automatic or manual.

 

In the dedicated robot automation concept the robot is a specialised automation component and integrated in the detailed handling of the other equipment components to a degree that makes it very difficult to re-program the robot for modified procedures.  

In flexible robot automation  (as QCX/RoboLab) the operator is automated rather than the equipment. The main automation element provided by the robot is the transport of samples between the different stations in the robot cell. The concept implies that the robot can easily be re-programmed or set up to service new equipment units.
 
The choice of automation concept depends on the complexity of a particular analysis method, the volume of the sample throughput and the overall automation concept desired. Typical key decision criteria to consider are :

  • Capacity and complexity of methods
  • Sample types and material properties
  • Analytical requirements    
  • Equipment location, building lay-out
  • Current and future labour costs
  • Daily operation and maintenance implications
  • Data processing requirements
  • Flexibility towards future needs 

 

In general the dedicated automated equipment solution (as QCX/AutoPrep) is - as graphically outlined in the diagram above - favorable with high sample throughput and/or low preparation complexity. For a ‘powder preparation only’ configuration, which is regarded as a low complexity operation, this means in most cases that a linear type arrangement is the most cost effective of the two alternatives.
Robotics solutions - flexible (as QCX/RoboLab) or dedicated - become preferable with increased number of preparation units serviced and with increased complexity of the procedures. This is because the robotics approach requires less adaptation of the equipment serviced and ‘simpler’ less expensive automation of a wider range of standard laboratory components. Other factors in favour of the flexible robotics concept are, as the name implies, it’s high flexibility towards future modifications and the ‘built-in’ manual back-up capability, since all equipment units serviced can also be serviced by a human operator. Complex sample preparations - for example fused bead preparation for XRF and sample dosing & weighing for Carbon/Sulphur/Moisture combustion analysis - are good examples of procedures for which a robotics based solution is the natural more flexible and less expensive solution 


QCX/RoboLab
QCX/RoboLab & AutoPrep

 

 

Application

QCX/RoboLab is a fully automated, robotics based laboratory concept with a very high degree of flexibility for individual solutions. The concept is based on sample preparation and laboratory equipment arranged in a circular configuration around a powerful industrial robot arranged in a  room with human access prohibited during operation. Analytical instruments are either located in an adjoining room, separated by a glass wall or integrated in the robotics circle. For the first mentioned set-up, sample loading takes place via transport belts and special loading components. These components may be eliminated when analytical equipment units are directly placed in the robotics circle. Key selection criteria for which lay-out concept to choose are available space, dust & noise levels and to what extent activities like off-line analysis, calibration, instrument check etc are best supported. 

Sample preparation and analysis equipment are sub-supplied from leading equipment suppliers, while FLSmidth as the system integrator designs and engineer the overall automation solution and produces the QCX/RoboLab software, integrated and engineered to the project specific configuration. Pending the automation specifications existing equipment may be integrated in the set-up. The system is software wise delivered as a completely integrated system, with efficient commissioning in mind. 

Samples arrive either via the connected automatic sample transport system or via manual/semi-automatic transfer points from the outside to the robot cell. Bar code scanning for identification of incoming samples is an available option.  A wide range of sample preparation and analysis tasks can be automated by the QCX/RoboLab system concept. Often applied preparation & analysis disciplines are:

 • crushing (and drying)  • particle sizing by laser or traditional sieving
 • splitting & dosing  • colour analysis
 • pressed powder and/or fused bead preparation for X-ray analysis  • combustion analysis for C/ S /H2O - determination
 • specific surface (Blaine)  • composite sample collection

Functionality

Incoming samples may be divided into several individual subsamples with individual preparation specifications; e.g. as an example: one portion for X-ray analysis, another for particle sizing by laser and the 3rd for collection of a shift composite sample. The only limitation to the number of sub-samples  is the available incoming sample quantity. 

Control of the individual components are normally undertaken via serial or network communication links, which supports  download of individual preparation parameters for various types of material. Via the same interfaces detailed operational status of the individual equipment units are picked up for display on the QCX system monitors. The QCX/RoboLab software provides a uniform and intuitive graphics & windows based user interface for all equipment units. It is developed with emphasis on one side simplicity and state-of-the-art software techniques, and on the other side robustness and reliability. One example of the these aspects is the easy-to-use definition of sample preparation methods, which at the same time is 100 % failsafe. As only legal and sensible options and sequences are accepted, it is impossible to define nonsense recipes like as an example 'routing a pressed powder tablet to a particle size analyzer'. 

The configuration normally also includes a small PLC for parallel signal interfacing. To the extent supported by the individual pieces of equipment, local operation is possible via built-in operator panels. Overall sequencing, priority handling and supervisory control is taken care of by the QCX/RoboLab software accessible from one or more QCX PCs. Mimic diagrams are provided for detailed monitoring of the system operation. 

The QCX/RoboLab software is delivered integrated in the project specific overall QCX system structure. At one end the integration with the QCX/AutoSampling module facilitates automatic transfer of sample ID and thereby sample preparation parameters for the incoming sample. At the analysis instrument end the QCX/Laboratory software  - with the full range of LIMS and reporting functionality - will control the analysis instruments and store the acquired analysis results in the QCX data base, eventually followed by automatic initiation of associated control calculations such as blending control.

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